AS MANY AS SIX SEQUENTIAL RUNS HAE BEEN USED IN SOME ANALYSES. AIR DRYING AND DESSICATION BETWEEN RUNS IS STANDARD. CARE SHOULD BE TAKEN TO SATURATE THE ATMOSPHERE OF THE RUNNING TANK BEFORE EACH RUN. RUNNING TECHNIQUES INVOLVE 24- TO 74-HOURS DESSICATION BY STANDARD METHOD. FOR GENERAL PURPOSES ROOM TEMPERATURES ARE SATISFACTORY. THE MOST SUCCESSFUL LIQUID PHASE CONSISTS OF 70 PARTS BY VOLUME OF ETHYL ACETATE, 35 PARTS ETHANOL, AND 30 PARTS DISTILLED WATER. ![]() THE SAME SOLID PHASE COATED ON ALUMINUM OR CLEAR ACETATE PLATES HAVE ALSO BEEN USED WITH EXCELLENT RESULTS. ![]() GLASS 20- BY 20-CM TLC PLATES WITH A 0.25-MM 1 LAYER OF SILICA GEL '60' WITHOUT FLUORESCENT INDICATOR ARE RECOMMENDED. USUALLY 1 TO 12 ONE-MM DISCS PUNCHED FROM THE TYPING TO BE ANALYZED ARE USED, DEPENDING ON THE DEGREE OF ANALYTICAL DETAIL REQUIRED. THE DYES ARE ELUTED DIRECTLY ONTO THE THIN LAYER PLATE STATIONARY PHASE BY PLACING THE 1-MM SAMPLE DISC DIRECTLY ONTO THE SPOTTING AREA OF THE TLC PLATE AND RUNNING THE ELUTION SOLVENT THROUGH THE SAMPLE DISC. THE MOST EFFICIENT ELUENT HAS BEEN FOUND TO BE 100 PERCENT PYRIDINE ADMINISTERED WITH DISPOSABLE MICROPIPETTES OF ONE TO TWO LAMBDA SIZE. A MORE RAPID DETERMINATION MAY BE MADE BY STUDYING RIBBON INK DYE TONERS OF THE TYPED IMPRESSIONS ON THE DOCUMENT IN QUESTION AND COMPARING THESE WITH DYES EXTRACTED FROM TYPING DONE ON THE SAME MACHINE ON A SERIES OF KNOWN DATES. HOWEVER, WITH SINGLE-ELEMENT TYPEWRITERS SUCH DEFECTS ARE USUALLY LIMITED TO ALIGNMENT CHANGES, THE STUDY OF WHICH MAY BE VERY COMPLEX AND TIME-CONSUMING. ONE APPROACH TO THE PROBLEM OF ESTABLISHING THE APPROXIMATE DATE ON WHICH A TYPED DOCUMENT WAS PREPARED HAS BEEN TO STUDY THE DEVELOPMENT OF TYPEWRITER DEFECTS OF A GIVEN MACHINE OVER CALENDAR TIME USING A DATED SERIES OF DOCUMENTS PREPARED ON THAT MACHINE.
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